Structure determination by NMR typically requires a protein concentration of 0.5 mM or greater, stable for several days at the desired temperature, usually 20-40 o C. Proteins and peptides should be ...

Please prepare your samples in the designated area or under a hood, and not on top of the magnet. The chemical shifts (d) of solvent signals observed for 1 H NMR and 13 C NMR spectra are listed in the ...

qNMR Using PULCON Use this document to perform quantitative NMR (qNMR) experiments using the PULCON methodology. This technique allows you to obtain concentration information about your NMR sample ...

This article establishes a neural network-based technique for automatic peak picking in 2D NMR spectroscopy, demonstrating a ...

All samples submitted for service must be accompanied by a completed submission form. The majority of users of the NMR 3 facility receive training and use the spectrometers independently. However, ...

Figure 5: a, Summary of the NMR data mapping unstructured or flexible ... containing 50 mM NaCl. Protein concentrations were determined by internally standardized amino acid analysis following ...

This means that you can setup any sample or samples to acquire multiple broadband nuclei, with no user intervention required (in terms of probe tuning or any changing of cables). The 300 is normally ...

If you have any needs for analysis of your samples with the high-field NMR instrumentation, do not hesitate to contact [email protected] (or [email protected]) for consultation and finding ...

Explore how external calibration ensures accuracy and long-term stability in quantitative qNMR methods for reliable ...

Its new workflow-oriented and intuitive user interface and optimized sample data management both provide a ... Billeter, J. Biomol. NMR, 2003. 27(2):p. 165-173) The new Dynamics Center is a ...