THF solution of borane-d 3 stabilized with N-isopropyl-N-methyl tert-butylamine used for the preparation of isotopically labeled alcohols.

开发了方便的BD 3 -THF配合物的制备方法。 某些胺可稳定BD 3 -THF以长期保存。 使用具有代表性烯烃的新型胺稳定BD 3 -THF进行了区域选择性研究。 烯烃的氢硼化为氧化后制备相应的氘代醇提供了方便的工具。 Convenient methods for the preparation of BD –THF complex were developed. Certain amines stabilize the BD –THF for long-term storage.

Borane-D₃ (D, 98%) (1 molar in THF) (+0.005M NaBD₄) Hover to zoom | Click to enlarge Synonyms (T-4)-Trihydro(tetrahydrofuran)boron; Borane, compound with tetrahydrofuran (1:1); (Tetrahydrofuran)borane; Borane-THF complex (1:1)

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One equivalent of BH 3 can hydroborate up to 3 equivalents of alkene. BH 3 -THF is the same as BH 3. Tetrahydrofuran (THF) is merely a solvent. Sometimes B 2 H 6 is written, which is another form of BH 3. It behaves in exactly the same way as BH 3. …

硼烷-d3-THF 络合物 溶液 1.0 M in THF, contains 0.005 M N-Isopropyl-N-methyl-tert-butylamine as stabilizer, 97.5 atom % D (mimimum); find Sigma-Aldrich-667714 MSDS, related peer-reviewed papers, technical documents, similar products & more at Sigma-Aldrich

2007年3月26日 · Regioselectivity studies were carried out with the new amine-stabilized BD 3 –THF with representative olefins. Hydroboration of olefins provides a convenient tool for making corresponding deuterated alcohols after oxidation. Convenient methods for the preparation of BD 3 –THF complex were developed.

BD 3 ·THF, stabilized with 0.005 mol% N-isopropyl-N-methyl-tert-butylamine (NIMBA), showed good thermal properties, directly resulting in improved reactant stability for deuterium label ...

2007年3月26日 · Regioselectivity studies were carried out with the new amine-stabilized BD3–THF with representative olefins. Hydroboration of olefins provides a convenient tool for making corresponding deuterated alcohols after oxidation. Convenient methods for the preparation of BD 3 –THF complex were developed.

2007年3月1日 · BD3·THF, stabilized with 0.005 mol% N-isopropyl-N-methyl-tert-butylamine (NIMBA), showed good thermal properties, directly resulting in improved reactant stability for deuterium label ...