
FT-IR characterization of supported Ni-catalysts: Influence of ...
2012年12月15日 · Supported Ni catalysts (2 wt.% Ni) were investigated by FT-IR and UV–vis-NIR spectroscopy, using CO 2, CH 3 CN and CO as probe molecules. The supports studied range from acidic (SiO 2), via amphoteric (Al 2 O 3, Mg(Al)O) to basic oxides (MgO, CaO).
An FTIR study of the dispersed Ni species on Ni-YSZ catalysts
2009年1月31日 · IR spectroscopy of low temperature adsorbed CO and CO + NO has been used to characterize the surface species on a 5% Ni-YSZ catalyst. Dispersed surface Ni species are present on the fresh catalyst, essentially formed by Ni 2+, although it is evident that these species are very easily reduced in very mild conditions to zerovalent atomic nickel ...
FTIR pattern of Nickel Oxide nanoparticles - ResearchGate
FTIR spectra of Nickel Oxide nanoparticles are shown in Fig. 2. The band observed at 1638 cm -1 is due to the OH bending of water. A strong band at 610 cm -1 is assigned to the Ni-O stretching...
Fourier transform infrared spectroscopy study of nanostructured nickel ...
2003年1月1日 · The present paper reports the Fourier transform infrared (FTIR) spectroscopic study of surface modes in nanostructured nickel oxide, having different average particle sizes ranging from 3 to 16 nm in the far IR region.
FTIR spectra of Ni (II)-complex (a) and β-Ni (OH)2 (b)
NiO nanosheets are prepared by calcination of nickel hydroxide nanosheets, obtained by the hydrolysis of trans-bis (acetato-κO)bis (2-aminoethanol-κ²N,O)nickel (II) complex. BET analysis reveals...
FTIR spectroscopy analysis of nickel nanoparticles. FTIR …
Characterization of obtained nickel-silicon dioxide (Ni-SiO2) nanocomposite was investigated using Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), Transmission/Scanning...
负载型镍催化剂的FT-IR表征:不同载体对金属相性能的影 …
FT-IR和UV-vis-NIR光谱法以CO 2,CH 3 CN和CO作为探针分子,对负载的Ni催化剂(Ni含量为2%)进行了研究。研究的载体范围从酸性(SiO 2)到两性(Al 2 O 3,Mg(Al)O)到碱性氧化物(MgO,CaO)。
FTIR Study of CO Adsorption on Ni−ZSM-5 - ACS Publications
2002年2月19日 · Adsorption of CO on Ni−ZSM-5 reveals the existence of two kinds of Ni 2+ ions, with the respective stretching frequencies being at 2220 and 2212 cm -1. The carbonyl complexes are resistant to evacuation at room temperature, which is explained by the high electrophilicity of cations in a ZSM matrix.
纳米结构氧化镍的傅里叶变换红外光谱研究。,Spectrochimica Acta …
2003年1月2日 · 合成具有3至16nm的不同平均粒径的纳米结构的氧化镍,并在远红外(IR)区域中记录样品的傅立叶变换红外(FTIR)光谱。 发现光谱由表面模式吸收主导,没有对应于本体横向光学模式的明显吸收。
Nickel oxide nanoparticles: Synthesis and spectral studies of ...
2013年12月1日 · Nickel oxide (NiO) nanoparticles were successfully synthesized by the reaction of nickel chloride with hydrazine at room temperature and thermal decomposition of the precursor nickel hydroxide (Ni(OH) 2) nanoparticles. The products were characterized by X-ray diffraction, Transmission electron microscopy, Fourier transform infrared spectroscopy ...
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