
Engineering catalyst supports to stabilize PdO - Nature
2021年10月18日 · We show that a 2D morphology of the PdO x phase synthesized with this approach is thermally stable and resistant to water poisoning, showing increased reactivity in methane oxidation.
Structural selectivity of supported Pd nanoparticles for ... - Nature
2019年1月28日 · In this study, two high-performance supported Pd nanoparticle catalysts (Pd/γ-Al 2 O 3 and Pd/zeolite-Y) are investigated for NH 3 -SCO using a combination of XAFS with DRIFTS and on-line mass...
(A) Pd K-edge FT-EXAFS spectra of ((a) PdO, (b) Pd foil, (c) Pd 1 Ag …
Figure 2 A displays the Fourier transform (FT) of k 3 -weighted extended X-ray absorption fine structure (EXAFS) data at the Pd K-edge of the Pd 1 Ag 2 solution, as well as results for reference...
XAFS数据分析和拟合.pdf 69页 - 原创力文档
2017年9月25日 · EXAFS数据处理的一般步骤 (1) 求 -E 曲线 (2) 边前背底扣除和数据归一化 (3) (E)背底扣除 0 (4) E k转换 各步骤顺序不是固定的, (5) 求 (k)及加权和加窗 也不都是必要的 (6) 快速Fourier变换 (7) Fourier滤波 (8) 曲线拟合,得到结构参数 EXAFS数据分析一般步骤 1.2 1.2 (a) ) (b) ) 0.8 u. 0.8 . u 0.4 a. . ( a Victoreen 0.4 ( 0.0 ) Modified Victoreen E ( -0.4 0.0 E 0 8800 9200 9600 10000 8800 9200 9600 10000 1.2 E (eV) 30 E (eV) (...
Elucidation of structure and nature of the PdO-Pd ... - PubMed
2013年6月14日 · The PdO-Pd phase transformation in a 4 wt% Pd/Al2O3 catalyst has been investigated using in situ X-ray absorption spectroscopy (XAS) and in situ X-ray total scattering (also known as high-energy X-ray diffraction) techniques. Both the partial and total pair distribution functions (PDF) from these re …
Overall information derived from XAS taking Pd metal and PdO as …
Overall information derived from XAS taking Pd metal and PdO as an example. (a) Schematic diagram of the X-ray absorption process, (b) normalized spectrum in energy space, (c) EXAFS spectrum in...
同步辐射XAFS数据处理干货,教你用同步辐射玩转材料科学!_同 …
2023年9月4日 · 其实XANES和EXAFS是对测出来的XAFS谱图能量区进行的一个划分,XANES (X-ray Absorption Near Edge Structure )是X射线近边吸收精细结构谱,而EXAFS (Extended X-Ray Absorption Fine Structure)是X射线延展边或者说拓展边吸收精细结构谱。 一般测试都是完整的XAFS谱。 以Cu-Foil为例,即以铜单质标样的XAFS谱为例来说, 以E0=8979ev为边,划分为三个区,如下图所示: 这样看是不是很清晰了呢?
CRESTS计划全球500 a以来的AMO与PDO重建数据报告
太平洋年代际震荡(pdo)与大西洋多年代际震荡(amo)作为全球年代际变化的主要模态,在全球气候变化研究中具有重要地位。 目前已有不少古气候记录用于重建过去500—1000 a以来的PDO和AMO变化。
Energy-Dispersive XAFS Studies on the Spontaneous Dispersion of PdO …
2004年5月20日 · Spontaneous dispersion and clustering processes of Pd were measured by means of the energy-dispersive EXAFS method. The spontaneous dispersion of bulky metal Pd into highly dispersed PdO was directly observed on the H-type zeolite in the atmosphere of O2.
保存和报告EXAF拟合数据 | Artemis | 同步辐射吸收谱(XAS)数据处 …
个人网站:https://twocircles24.com/ 继续之前多壳层拟合的Cr2O3数据案例来保存拟合数据并在Originlab画图,再按照发文章的标准把完整的一套EXAFS数据(一张k空间,一张R空间,一 …
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