Small, but powerful and attractive: 19 F in biomolecular NMR
2022年1月6日 · This perspective summarizes the unique benefits of solution and solid-state 19 F NMR spectroscopy for the study of biological systems. Particular focus is on the most recent …
19 F Solid-state NMR characterization of pharmaceutical solids
2022年8月1日 · We aim to review recent advancements of 19 F magic angle spinning NMR methods in modern drug research and development. Applications to polymorph screening at …
solid state NMR. In this technique, polarization from abundant spins such as 1H or 19F is transferred to dilute spins such as 13C or 15N. The overall effect is to enhance S/N: 1. Cross …
19F Solid-State Nuclear Magnetic Resonance Spectroscopy
Solid-state 19 F-NMR is a valuable tool in structural studies of membrane-associated peptides. Progress in this area became possible after successful design and synthesis of the fluorine …
Solid-state NMR spectroscopy - PMC - PubMed Central (PMC)
Solid-state nuclear magnetic resonance (NMR) spectroscopy is an atomic-level method used to determine the chemical structure, three-dimensional structure, and dynamics of solids and …
Enlarging the scenario of site directed 19 F labeling for NMR
2023年12月12日 · The 1D 19 F NMR spectrum of GB1 shows the presence of one well defined main peak and two smaller peaks (Fig. 3b), exhibiting different features, both in terms of shape …
Solid-State NMR 19F–1H–15N Correlation Experiments for …
2022年9月23日 · Several solid-state NMR techniques have been introduced recently to measure nanometer distances involving 19 F, whose high gyromagnetic ratio makes it a potent nuclear …
Interface-edited solid-state NMR to study cell interfaces
2025年3月22日 · Takahashi, H. et al. Solid-State NMR on bacterial cells: selective cell wall signal enhancement and resolution improvement using dynamic nuclear polarization. J. Am. Chem. …
Solid-state (19)F-NMR of peptides in native membranes
A particularly successful structural method is solid-state NMR, which makes use of macroscopically oriented lipid bilayers to study selectively isotope-labelled peptides. Native …
Solid-State 19F NMR Chemical Shift in Square-Planar …
2023年3月15日 · The 19 F NMR chemical shifts of the monomers in solution (1pF-m (solv), 1oF-m (solv), and 3F-m (solv)) were calculated using the geometries optimized with the SMD …