2017年2月1日 · Applications of NMR spectroscopy in starch research are summarized. NMR spectroscopy probes structural basis of physical behaviours of starch systems. Various types of NMR techniques reveal different aspects of starch structures. Results of NMR spectroscopy correlate well with those of other analytical methods.

2011年5月24日 · A novel, fast, and straightforward procedure is presented for the characterization of starch (the largest energy component in food) and modified starches (such as octenyl succinic anhydride (OSA)-modified starches used as a dispersing agent in the food industry).

2014年1月1日 · Nuclear magnetic resonance (NMR) spectroscopy is a major tool for the analysis of both chemical and physical properties of starches and starch-containing systems. At the molecular level, high-resolution NMR is the method of choice for defining the degree of branching of starch polysaccharides in solution.

In the 1 H NMR spectrum of native starch (Fig. 4a), the signals at 3.3 and 2.5 ppm were assigned to hydrogen atom of the solvent DMSO. As expected, the peaks recorded between 4.5 and 5.5 ppm...

This article aims to provide a comprehensive and critical review of research characterizing starch-based materials using solid-state NMR, and to briefly introduce the most advanced and promising NMR strategies and hardware designs used to overcome the sensitivity and resolution issues involved in structure–function relationships.

2016年9月7日 · We show that considerable molecular detail of starch fragmentation can be obtained from multivariate analysis of spectral features in optimized 1 H– 13 C NMR spectroscopy of starch fragments to identify relevant features that distinguish processes in starch utilization.

2016年10月1日 · NMR spectroscopy has been used to investigate the properties of various starch systems. These include chemical composition, physical and chemical structures, gelatinization, retrogradation,...

Using two-dimensional (2D) high resolution solid-state nuclear magnetic resonance (SS-NMR) on 13 C-labelled starches that were obtained from Chlamydomonas reinhardtii microalgae, we established a complete and unambiguous assignment for starch and its constituents (amylopectin and amylose) in the two crystalline forms and in the amorphous state.

2017年2月1日 · Applications of NMR spectroscopy in starch research are summarized. NMR spectroscopy probes structural basis of physical behaviours of starch systems. Various types of NMR techniques reveal different aspects of starch structures. Results of NMR spectroscopy correlate well with those of other analytical methods.

2014年3月1日 · Nuclear magnetic resonance (NMR) spectroscopy is a major tool for the analysis of both chemical and physical properties of starches and...