2020年6月3日 · 1D 1H NMR with on non-deuterated solvents (“no-D”) Without deuterium, the magnet field cannot be locked and on our older magnets, the field moves with each scan. Because of this, 1H NMR without deuterium lock only works well on two NMR instruments: the 400SL and the 500 Ascend. 1. The lock and sweep must be off.

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Shimming on non-deuterated solvents (“no-D”) Automatic Shimming + First run a one scan 1D proton spectrum without locking, so that you know where the solvent peak occurs. Use ns of 1 and ds of 0. Do [tune], [prosol], [gain], [go]. The following procedure will tell the instrument to not lock on deuterium, but use the proton signal

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No deuterium (no-D) NMR is a technique that can be a useful alternative to using expensive deuterated solvents, if you are working with a neat sample, or want to directly monitor a reaction mixture.

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2023年7月31日 · No-D NMR is a practical and powerful way of detecting water and other additives in organic solvents. It provides an alternative when Karl Fischer titrations are unavailable or this level of accuracy is unnecessary.

No-D NMR (No-Deuterium Proton NMR) technique is a measurement of high resolution 1 H NMR spectra without deuterium solvent. It suggests that any reaction mixture or reagent solution are directly available for No-D NMR measurement.

2022年3月1日 · ONM 患者定义为：CT（短轴直径 < 1 cm）和 PET（标准化摄取值 < 2.5）均未怀疑淋巴结受累，但术后病理结果为转移的患者。 通过 K-M 生存曲线以及 Cox 比例风险回归模型来评估患者预后生存及危险因素。 通过总生存时间（OS）和无复发生存时间（RFS）来比较临床确定的淋巴结转移患者和合并 ONM 患者的生存预后，以及评估接受辅助治疗的 ONM 患者的生存获益情况。 图 1：研究设计流程图. 结果. 01 基线特征. 入组患者的临床病理特征见表 1。 在术 …