XPS Spectra Antimony (Sb) Compounds The XPS Spectra section provides raw and processed survey spectra, chemical state spectra, BE values, FWHM values, and overlays of key spectra. Atom% values from surveys are based on sample, as received, and Scofield cross-sections. Atom% values are corrected for IMFP and PE.

2011年4月5日 · Synchrotron-based energy resolved XPS was used to characterize the structure of IrO2 RuO2-coated Sb2O5 SnO2 nanoparticles. Samples were heat treated at 300, 350, 400, 450 and 500 °C after chloride Ir...

2000年2月18日 · X-ray photoemission spectroscopy (XPS) was carried out at the beamline 4B9B of the Beijing Synchrotron Radiation Facility for the antimony oxides in the organosol before heating. XPS shows that the Sb 3+ ions make a dominant contribution.

X-ray photoelectron spectroscopy (XPS or ESCA) curve fitting procedures, reference materials and useful notes are listed here to provide a starting point for the consistent interpretation of XPS spectra. These reference pages contain tips and techniques that are designed to help both the novice and advanced XPS user.

XPS 和 AES 已应用于氧化锑、Sb2O3、Sb2O4 和 Sb2O5 的表面分析。 通过计算机操作的氧和锑贡献的分离，发现根据 XPS 数据计算的氧与金属原子比接近预期值。 发现锑粉末样品被 Sb2O4 表面层覆盖，并且显示和讨论了深度剖析期间 Sb 的俄歇 MNN 峰形状的变化。 XPS 和 AES 已应用于氧化锑、Sb2O3、Sb2O4 和 Sb2O5 的表面分析。 通过计算机操作的氧和锑贡献的分离，发现根据 XPS 数据计算的氧与金属原子比接近预期值。 发现锑粉末样品被 Sb2O4 表面层覆盖， …

基于同步加速器的能量分辨XPS用于表征IrO 2 -RuO 2 包覆的Sb 2 O 5 ―SnO 2 纳米颗粒的结构。 在将氯化物 Ir 和 Ru 前体添加到 Sb 2 O 5 -SnO 2 后，样品在 300、350、400、450 和 500°C 下进行热处理。

XPS 谱图解读. Sb3d 具有明显的自旋轨道分裂峰（Δ=9.39 eV）。 金属锑的峰形大致对称。 Sb3d 5/2 和 O1s 峰之间直接重叠。 使用未与 O1s 产生重叠的 Sb3d3 峰进行拟合。 Sb3d5 峰的强度和结合能出峰位置由 Sb3d3 峰根据自旋轨道分裂峰强度比确定。

XPS and AES have been applied to the surface analysis of antimony oxides, Sb 2 O 3, Sb 2 O 4 and Sb 2 O 5. By means of the computer-operated separation of oxygen and antimony contribution, the oxygen to metal atomic ratios calculated from XPS data were found to be close to the expected values.

For pristine materials, rectangular-shaped LNMO exhibited stable cycle retention at room temperature compared with pentahedron-shaped LNMO owing to the Mn 3+ content that provides excellent...

Synchrotron-based energy resolved XPS was used to characterize the structure of IrO2 RuO2-coated Sb2O5 SnO2 nanoparticles. Samples were heat treated at 300, 350, 400, 450 and 500 °C after chloride Ir and Ru precursors were added to Sb2O5 SnO2.