In this study, SnS/NC composite was successfully synthesized by using one-pot hydrothermal and annealing methods, and whose electrochemical storage performance was also investigated.

2020年4月15日 · Cubic polymorph of SnS (SnS-CUB) shows a remarkable structural stability up to 400 °C. The structural transition of SnS-CUB to orthorhombic SnS occurs at 450 °C. Three distinct regions of weight loss are observed in TGA of cubic SnS nanoparticles; around 300 °C, 600 °C and 800 °C.

2007年9月30日 · Nanorods and nanosheets of tin sulfide (SnS) were synthesized by a novel thioglycolic acid (TGA) assisted hydrothermal process. The as prepared nanostructures were characterized by X-ray diffraction (XRD) study, scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

SNs with high specific surface area were silanized by two complementary mechanisms using organosilanes with different functionalities, 3-methacryloxypropyltrimethoxysilane (MPS), octyltrimeth......

TGA and DTG profiles of bare SnS, RGO, and SnS-RGO composites. [...] A simple, green, and ultra-fast one-pot supercritical ethanol (scEtOH) route was developed to synthesize tin...

2021年3月24日 · We present our work on the rapid hydrothermal synthesis of highly crystalline 2D SnS nanostructures. An innovative idea is used in which thioglycolic acid is the sulfur precursor source. Structural studies indicate the material has grown in …

摘要 通过新型巯基乙醇酸 (TGA) 辅助水热法合成了硫化锡 (SnS) 纳米棒和纳米片。 通过 X 射线衍射 (XRD) 研究、扫描电子显微镜 (SEM) 和透射电子显微镜 (TEM) 表征所制备的纳米结构。

2007年9月30日 · Nanorods and nanosheets of tin sulfide (SnS) were synthesized by a novel thioglycolic acid (TGA) assisted hydrothermal process. The as prepared nanostructures were characterized by X-ray diffraction (XRD) study, scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

In this paper, we employed a simple and cost-effective thioglycolic acid (TGA) free hydrothermal method, based on thiourea hydrolysis of stannous chloride dihydrate [SnCl 2.2H 2 O] at 160 ∘ ∘ C–190 ∘ ∘ C for 6 h, for the synthesis of SnS nanoparticles.

2006年9月1日 · In this paper, a simple thioglycollic acid (TGA) assisted hydrothermal synthesis route for novel SnS nanoflowers is reported, and the characterization and properties of the product are presented.