实验信息 如果样品中的氯浓度高，Mg1s 峰将与 Cl LMM 俄歇峰高度重叠。 首选采集 Mg2s 和/或 Mg2p 区域而不是 Mg1s 峰。 XPS 光谱解读 Mg1s 峰通常在 300 eV-390 eV 处伴有俄歇峰。 如果镁颗粒表层被覆盖（例如，被碳层覆盖），即使未观察到 Mg1s 峰，也可以观察到 Mg KLL 俄 ...

It may preferable to acquire Mg2s and/or Mg2p regions instead of the Mg1s peak. Interpretation of XPS spectra Mg1s peak often accompanied by Auger peaks between 300eV-390eV. If magnesium is buried (under carbon, for example), Mg KLL Auger peaks may be observed even if Mg1s is not (due to difference in electron kinetic energy).

The XPS spectra of Mg 1 s (Fig. 4b) exhibited two distinct peaks with shifting to high binding energy (B.E), which are further assigned at 1306.39 eV and 1307.75 eV, respectively.

In the case of Mg 1s xps fine spectra shown in Fig. 4d, there exists only a single peak with a binding energy value of 1303.9 eV which is attributed to Mg 2+ species in MgO or Mg (OH) 2 [76]....

有Mg1s就肯定有Mg2s和Mg2p，只不过在Al alpha X-ray能量（1486.7eV)下，Mg1s的电离截面（与x-ray光子作用几率）比Mg2s和2p要高几十倍。 你的Mg1s cps大概有7000，所以Mg2p cps理论上应该只有200-300左右。 如果检测器不够好，是容易融入背景噪音的。 10 0条评论 举报 酒肆 …

Data Collection Settings for Magnesium (Mg) Conductivity: Magnesium readily develops a native oxide that is sensitive to Flood Gun – Differential Charging Possible – float sample recommended Primary Peak (XPS Signal) used to measure Chemical State Spectra: Mg (1s) at 49.6 eV

A simple solution combustion method is used to synthesize spinel type MgFe2O4 (MFO) and CoCr2O4 (CCO) oxides, which are combined with the mechanical mixing method to construct a Z‐scheme MFO/wt%CCO...

可以将范围采到1350eV，这样的话，就可以看到Mg1s峰位有没有出现，可能更好的帮助你对Mg进行定量， 45eV附近的峰位是Ca3s，52左右的峰位应该不是Mg2p，没有这么强的信号，难道样品中含有Se？

1997年10月1日 · XPS measurements have been performed on a series of Mg II salts (NO 3−, CO 32−, SO 42−, Cl −, CH 3 COO −), hydroxides and oxides, these latter compounds are both commercial and prepared in laboratory.

It may preferable to acquire Mg2s and/or Mg2p regions instead of the Mg1s peak. Interpretation of XPS spectra Mg1s peak often accompanied by Auger peaks between 300eV-390eV. If magnesium is buried (under carbon, for example), Mg KLL Auger peaks may be observed even if Mg1s is not (due to difference in electron kinetic energy).